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The structure of the cobalt present in carbon-supported Co and Co-Mo sulfide catalysts was studied by means of X-ray absorption spectroscopy at the Co K-edge and by X-ray photoelectron spectroscopy (XPS). Thiophene hydrodesulfurization activities were used to measure the catalytic properties of these catalysts. By comparison of the EXAFS and XANES spectra of the catalysts with those of c09sS and Cos2 model compounds, it was concluded that all Co atoms in a catalyst prepared with nitrilotriace...