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Carbone, Giorgio; Burnley, James; Moses, John E. (2013)
Publisher: Thieme Chemistry
Languages: English
Types: Article
Subjects:
The reduction of a range of substituted azidonitrobenzene derivatives to the corresponding aniline is described. The chemoselective reaction proceeds cleanly and in good yield, generating minimal waste products. The process involves a thiazolium salt derived species which is proposed as a radical anion relay, with tert-butoxide as the stoichiometric reductant.
  • The results below are discovered through our pilot algorithms. Let us know how we are doing!

    • Acquisition Time (sec) 3.9846 Comment Slot No. 38 Sample ID gc4-38-1 SupervisorID moses Lab Phone No. 13540 UserID g_car Date 05 Apr 2012 11:12:16 Date Stamp 05 Apr 2012 11:12:16 File Name \\brukdpx400\nmr_data\G_CAR\NMR\G_CAR.GC4-38-1\6\PDATA\1\1R Nucleus 1H Number of Transients 16 Origin dpx400 Owner nmruser Points Count 65536 Pulse Sequence zg30 SW(cyclical) (Hz) 8223.68 Solvent DMSO-d6 Spectrum Offset (Hz) 2465.2061 Sweep Width (Hz) 8223.56 Temperature (degree C) 25.000 Acquisition Time (sec) 3.4210 Comment Date 04 Apr 2012 07:09:04 File Name \\brukav400\nmr_data\G_CAR\NMR\G_CAR.GC4-50-1\1\PDATA\1\1R Nucleus 1H Number of Transients 16 Owner nmruser Points Count 32768 SW(cyclical) (Hz) 4789.27 Solvent DMSO-d6 Sweep Width (Hz) 4789.13 Temperature (degree C) 25.160
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