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fbtwitterlinkedinvimeoflicker grey 14rssslideshare1
Evans, Robert; Day, Iain J. (2016)
Publisher: Royal Society of Chemistry
Languages: English
Types: Article
Subjects: QD0071, QD0450
Diffusion NMR is a potentially routine tool in the analysis of mixtures, from industrial and synthetic outputs to natural products. However, the technique struggles to resolve species of similar size. Matrix-assisted DOSY offers a flexible approach to resolving such ambiguities on the basis of the chemical structures involved and on their interactions with a larger co-solute or matrix. The use of chromatographic supports, surfactants and polymers, in particular, is illustrated. The resolution of a wide range of different analyte mixtures, on the basis of differences in chemical structure and in stereochemistry, is demonstrated.
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