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Publisher: Beilstein-Institut
Journal: Beilstein Journal of Organic Chemistry
Languages: English
Types: Article
Subjects: Full Research Paper, Chemistry, Organic Chemistry, ester, N-alkylation, imidazol-1-yl-acetic acid hydrochloride, zoledronic acid
Summary A convenient and practical synthesis of imidazol-1-yl-acetic acid hydrochloride was achieved via N-alkylation of imidazole using tert-butyl chloroacetate followed by a non-aqueous ester cleavage of the resulting imidazol-1-yl-acetic acid tert-butyl ester in the presence of titanium tetrachloride. The synthesized imidazol-1-yl-acetic acid hydrochloride was then utilized to prepare zoledronic acid.
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